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A rapid and reliable assay to determine flumequine, marbofloxacin, difloxacin, and sarafloxacin in commonly consumed meat by micellar liquid chromatography

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A rapid and reliable assay to determine flumequine, marbofloxacin, difloxacin, and sarafloxacin in commonly consumed meat by micellar liquid chromatography

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dc.contributor.author	Peris Vicente, Juan
dc.contributor.author	Iborra-Millet, Jesús Javier
dc.contributor.author	Albiol-Chiva, Jaume
dc.contributor.author	Carda Broch, Samuel
dc.contributor.author	Esteve i Romero, Josep-Salvador
dc.date.accessioned	2023-11-20T14:24:55Z
dc.date.available	2023-11-20T14:24:55Z
dc.date.issued	2019
dc.identifier.uri	https://hdl.handle.net/10550/91260
dc.description.abstract	BACKGROUND: Micellar liquid chromatography - fluorescence detection was used to determine the antibiotics flumequine, marbofloxacin, difloxacin, and sarafloxacin in porcine, bovine, poultry, ovine, caprine, rabbit, and equine meat, to verify compliance with EU Regulation 37/2010 with regard to the occurrence of veterinary drugs in food. RESULTS: The analytes were isolated from the matrix by ultrasonication-assisted leaching in a micellar solution, and the supernatant was filtered and directly injected. The fluoroquinolones were resolved in < 19 min using a C18 column, with an isocratic mobile phase of 0.05 mol L−1 sodium dodecyl sulfate - 8% 1-butanol - 0.5% triethylamine buffered at pH 3. The limits of quantification (0.01-0.05mgkg−1) were below the maximum residue limits (0.15-0.4mgkg−1). The method was validated by EU Commission Decision 2002/657/EC guidelines. CONCLUSION: The method shows practical advantages such as simplicity, lowcost, eco-friendliness, safety, and applicability for routine analysis, and is useful for surveillance programs.
dc.language.iso	eng
dc.relation.ispartof	Journal of the Science of Food and Agriculture, 2019, vol. 99, num. 3, p. 1375-1383
dc.source	Peris Vicente, Juan Iborra-Millet, Jesús Javier Albiol-Chiva, Jaume Carda Broch, Samuel Esteve i Romero, Josep-Salvador (2019). A rapid and reliable assay to determine flumequine, marbofloxacin, difloxacin, and sarafloxacin in commonly consumed meat by micellar liquid chromatography. Journal of the Science of Food and Agriculture 99 3 1375 1383. https://doi.org/10.1002/jsfa.9314
dc.subject	farmacologia veterinària
dc.subject	aliments adulteració i inspecció
dc.title	A rapid and reliable assay to determine flumequine, marbofloxacin, difloxacin, and sarafloxacin in commonly consumed meat by micellar liquid chromatography
dc.type	journal article
dc.date.updated	2023-11-20T14:24:56Z
dc.identifier.doi	10.1002/jsfa.9314
dc.identifier.idgrec	132359
dc.rights.accessRights	open access